Properties of Ni3Fe Nanoparticles Prepared by Chemical Method |
K. Zábranský, O. Schneeweiss, N. Pizůrová and B. David
Institute of Physics of Materials, Academy of Sciences of the Czech Republic, Žižkova 22, CZ-616 62 Brno, Czech Republic |
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Ni3Fe nanoparticles prepared by calcination of the iron-nickel oxalate were investigated by X-ray diffraction, Mössbauer spectroscopy and magnetic measurements. The high temperature X-ray diffraction shows two stages of transformation of oxalate: (i) amorphization and (ii) formation of nanocrystalline Ni3Fe particles. The development of coercivity, magnetization and mean coherence length ( ≈ particle size) is discussed. |
DOI: 10.12693/APhysPolA.118.785 PACS numbers: 61.05.cp, 61.46.-w, 75.20.En, 75.50.Bb |