Laboratory Dispersive EXAFS Spectrometer |
A. Mosset, P. Lecante, P. Baules, J. Jaud, J. Galy CEMES-CNRS, 29 rue Marvig, BP 4347, 31055 Toulouse, France and A. Burian Institute of Engineering Problems, University of Silesia, Śnieżna 2, 41-200 Sosnowiec, Poland |
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We report on a laboratory EXAFS spectrometer optimized for transmission dispersive mode. Absorption edges ranging from 6 to 20keV can be studied. Factors determining energy range and resolution are detailed. A new asymmetric geometry which allows to use all the lattice planes of the dispersing crystal is described and the choice of the best plane analysed. EXAFS spectra of Cu metal and Cu acetate, obtained on this laboratory facility, are compared to the corresponding spectra recorded on the French synchrotron facility (LURE). |
DOI: 10.12693/APhysPolA.91.825 PACS numbers: 61.10.Ht, 07.85.Nc, 61.43.-j |