Influence of Annealing Conditions on Magnetic Properties and Phase Constitution of the Rapidly Solidified Fe65Pr9B18W8 Alloy Ribbons |
K. Filipeckaa,b, P. Pawlik a, A. Kozdraś c and J. Filipecki b
aInstitute of Physics, Faculty of Production Engineering and Materials Technology, Częstochowa University of Technology, al. Armii Krajowej 19, 42-200 Częstochowa, Poland bInstitute of Physics, Faculty of Mathematics and Natural Science, Jan Długosz University, al. Armii Krajowej 13/15, 42-200 Częstochowa, Poland cDepartment of Physics, Faculty of Production Engineering and Logistics, Opole University of Technology, Ozimska 75, 45-370 Opole, Poland |
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In the present work, the influence of annealing conditions on magnetic properties and phase constitution of the rapidly solidified Fe65Pr9B18W8 alloy ribbons, were investigate. Samples were prepared by arc-melting of high purity constituent elements under the Ar atmosphere. Ribbons were obtained by melt-spinning technique under low pressure of Ar. The ribbons in as-cast state had amorphous structure and soft magnetic properties. Heat treatment, carried out at various temperatures (from 923 K to 1023 K) for 5 min, resulted in an evolution of the phase constitution that caused changes in magnetic properties of the alloy. The crystallization behavior was studied using differential scanning calorimetry and X-ray diffractometry. The room temperature magnetic properties were determined from hysteresis loops measured by VSM magnetometer in the external magnetic field up to 2 T. |
DOI: 10.12693/APhysPolA.129.185 PACS numbers: 75.50.Ww, 75.50.Kj, 71.20.Eh |