Phase Composition and Magnetic Properties of the Nanocrystalline Fe64.32Pr9.6B22.08W4 Alloy

K. Filipecka, K. Pawlik, P. Pawlik, J. J. Wysłocki, P. Gębara, A. Przybył Institute of Physics, Faculty of Materials Processing, Technology and Applied Physics, Czestochowa University of Technology, Armii Krajowej 19, 42-200 Czestochowa, Poland

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The aim of the present work was to study the influence of annealing conditions on magnetic properties and the phase constitution of rapidly solidified Fe64.32Pr9.6B22.08W4 alloy ribbons. The base alloy was prepared by arc-melting of the high purity elements under an Ar atmosphere. Subsequently the ribbon samples were obtained by melt-spinning technique under low pressure of Ar. In order to develop nanocrystalline structure, the samples were annealed at 1003 K for 5, 10, 20 and 30 min. The room temperature magnetic properties were determined from hysteresis loops measured by VSM magnetometry in the external magnetic field up to 2 T. For comparison the influence of annealing temperature on magnetic properties was studied for the same alloy composition. The ribbons were annealed at temperatures from 929 K to 1023 K for 5 min. X-ray diffractometry was used to determine the phase composition of annealed ribbons. Heat treatment resulted in an evolution of the phase constitution, that caused changes in magnetic properties of the alloy.

DOI: 10.12693/APhysPolA.126.164 PACS numbers: 75.50.Ww, 75.50. Kj, 71.20.Eh